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Thread: How to Isomerise THC - making the THC Acetate.

  1. #1
    420 Member Medical Marijuana's Avatar
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    How to Isomerise THC - making the THC Acetate.

    isomerising!!!!!

    Dissolve the hash oil in absolute ethanol or pure methanol in the ratio
    of one gram extract to ten grams solvent. There must be no water in
    this solution, as the next step is the addition of one drop of 100%
    sulfuric acid per gram of extract. Add the acid slowly, drop by drop,
    stirring slowly and completely, with a long glass stirring rod. Place a
    Pyrex pot containing the extract-alcohol-acid solution into the
    refluxing apparatus and reflux for two hours. The acid will not
    evaporate and will remain in the Pyrex pot. Allow to cool. Take the
    cooled solution, pour with an equal volume of water and 1/2 volume of
    petroleum ether into the ether-extraction apparatus (separation funnel).
    Allow to settle, and drain the ether extract layer. This leaves an
    ether-extract-acid mix from which the acid must be purged. To
    accomplish this, pour the ether-extract-solution into four volumes of 5%
    sodium bicarbonate solution (1 gram bicarb. in 20 grams of water). This
    will neutralize the acid, releasing CO2 and leaving a solution of sodium
    sulphate. Allow this to settle into layers, then drain the
    ether-extract layer. Mix the ether-extract solution with an equal
    volume of pure water and let it separate. Drain off the ether-extract
    layer. Evaporate the ether and what remains is hash oil in which all of
    the cannabinoids have been converted into THC
    Oh my, having just typed all this in, I thought to check my copy of
    "Cannabis Alchemy" for a method. Not only does it concur with this
    method of isomerization, it has lots of whiz hints on fractionally
    distilling hash oil to get an ultra-pure product. It also claims that
    if you convert THC to its acetate, it becomes very potent and
    psychedelic.

    WARNING

    Before boiling petrols and ether - Get a flow hood with external venting.

    Confirm via GCMS there is no adulterants left in your "purified" product.

    Make sure all motors are brushless, no homebrew crap, including flowhood.

    Similiar in theory to FLIR, TDT air scans can be done around the home to alert to the presence of various compounds used in chemistry. Unlike FLIR -
    this does not require a warrant since it is the ambient air around said lab, is completely non invasive and a dead giveaway.

    Or just grow the green, ditch the chemistry.

  2. #2
    420 Member FreakNature's Avatar
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    Re: How to Isomerise THC - making the THC Acetate.

    You forgot "Kids, don't try this at home". A good resource to test for residual adulterants is "Gas Chromatic Mass Spectrometers R Us" in the phone book. Sorry - couldn't help myself.

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