Run lower proof drinking alcohol through the Green Oil Machine twice and you'll be around 190 proof. What's left in the pot is water.i cannot get my hands on anything stronger then 75.5% food grade or i would opt for that.
I CAN NOT GET IT ANYMORE..Gets pretty expensive to have to keep buying special solvent if you don't recapture it.
Turn off your caps lock delta!
And if you recaptured it you would still have some .
If you can't get it it doesn't do you a lick of good. And certainly wouldn't be as helpful for someone to write a tutorial on how to do it if it's that hard to get.
Did you follow all the steps here:
Seem pretty complicated to be done safely.
its banned in canada .. unless a lab or university etc.. with cause to use.. rcmp will visit.. be nice to have a liter to
cook up a personal batch of wickly good oil..
the pet e is use to extract the cannabinniods out of the ethanol extra solution .. with water .. add
in a separatory funnel add water ethanol soln and pet e .. shake a little release gas!!!!!!!!!!!!!!!! shake again
release gas!!! .. lets stand 5 mins the layers separate keep the top.. could wash middle layer again twice..
evaporate off bingo deadly oil.. clean of crap..
i would use this apparatus!! for ethanol or methanol oil extraction from the pot..
do not use iso..
stonylab 500ml Soxhlet Type Extraction Apparatus, 24/29 Borosilicate Glass Soxhlet Extractor with Allihn Condenser and Two 500 ml Flat Bottom Flasks
should be round bottom flash for heat with a few boiling chips.. self enclosed system ..
with condenser and running cold water ..
use water heat..
now there is a secrete step if you want to see god.. i could tell you about ?
You don't need a soxhlet rig to get great oil. I use naphtha/pet.ether I get from distilling Coleman's Camp Stove fuel. Then I use the same still to recover almost all the solvent and finish off the oil in a pyrex pie plate on a pot of simmering water. No hit of smell of the naphtha and that stuff is stinky. The wet used pot I put back into the still and cook off the solvent trapped in it for about a 90% recovery overall. Got to be Coleman's tho. Almost 10 degree lower bp than the cheaper shit.
My still is a glass bottle that holds 4L and I have a 1.5 L one I use for the recovery.
Crappy picture but the bottle is sitting in a big stock pot as a water bath with a separator under the glass bottle and boiling chips inside of course. Rubber stopper for the thermometer and the 3/8" copper tube that runs to my condensor which is the same tubing inside a coffee can so a 2L pop bottle full of frozen salted water fits in nicely. I keep a few of those in the freezer ready to do a run. Automotive anti-freeze in the can. Water rusts those out fast. Ask me how I know.
I've made booze with it too from a simple sugar mash. Excuse the clutter.
Is the secret step maybe . . . isomeration? I have the glassware, chems, training and the procedure to do that too but haven't got around to it yet. Soon tho.
what temp does the pet ether boil over ? how much u get out of 3.87 liter can coleman camp fuel?
i dont think that is USP grade pet ether .. close the residual from the usp stuff be very low .0002% or less
might be .0001%
thats us pharmacopeia.. standards for testing chemicals etc. .. either that or the bp.. british pharmacopeia.. pretty much covers everything ..